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Kev soj ntsuam zoo rau kev xa khoom sai thiab siab Purity CAS 93-02-7 2, 5-Dimethoxybenzaldehyde


  • Cas:93-02-7 ib
  • Molecular formula:C9H10O3
  • Molecular Luj:166.17 Nws
  • EINECS:202-211-5
  • Synonyms:2,5-Dimethoxybenzaldehyde, 97%; 2,5-Dimethoxybenzald; 5-DiMethoxybenzaldehyde; 2,5-DiMethoxybenzaldehyde, Tshuaj Phau Ntawv 97% 25GR; NSC6315; 93-02-7; 2,5-DimethoxybenzaldehydeVetec(TM) reagentgrade, 98%; 2,5-DIMETHOXYBENZALDEHYDE
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    Khoom cim npe

    Peb mob siab rau kev ua tau zoo, muab kev pabcuam rau cov neeg siv khoom”, vam tias yuav dhau los ua pab pawg kev koom tes zoo tshaj plaws thiab tus thawj tswj hwm kev lag luam rau cov neeg ua haujlwm, cov chaw muag khoom thiab cov neeg siv khoom, paub txog tus nqi sib koom thiab txuas ntxiv mus rau Kev Tshuaj Xyuas Zoo rau Kev Xa Khoom sai thiab Siab Purity CAS 93-02-7 2, 5-Dimethoxybenzaldehyde, Peb yuav muab cov khoom zoo tshaj plaws zoo tshaj plaws, muaj peev xwm ua tau zoo tshaj plaws ntawm cov nqi hnyav, rau txhua tus neeg siv khoom tshiab thiab qub nrog tag nrho cov kev pabcuam ntsuab zoo tshaj plaws.
    Peb mob siab rau kev ua tau zoo, muab kev pabcuam rau cov neeg siv khoom ", vam tias yuav dhau los ua pab pawg kev koom tes zoo tshaj plaws thiab tus thawj tswj hwm kev lag luam rau cov neeg ua haujlwm, cov neeg muag khoom thiab cov neeg siv khoom, paub txog tus nqi sib koom thiab kev txhawb nqa txuas ntxiv rauTuam Tshoj Chemical Intermediates thiab Pharmaceutical Raw Materials, Vim muaj kev hloov pauv hauv daim teb no, peb koom nrog peb tus kheej rau hauv cov khoom lag luam nrog kev mob siab rau thiab kev tswj hwm zoo. Peb tuav lub sijhawm xa khoom raws sijhawm, tsim qauv tshiab, zoo thiab pob tshab rau peb cov neeg siv khoom. Peb lub moto yog xa cov kev daws teeb meem zoo hauv lub sijhawm teev tseg.

    2,5-Dimethoxybenzaldehyde yog lub teeb daj crystalline hmoov nrog ib qho hnyav molecular ntawm 166.18 thiab qhov kub ntawm 146 ° C. Nws yog soluble hauv cov kuab tshuaj organic xws li ethanol thiab ether. Nws yog tsuas yog siv los ua tshuaj nruab nrab.

    Yam khoom

    STANDARD

    Qhov tshwm sim

    Grey rau daj khoom

    NMR

    Ua raws

    Purity

    > 98%

    Melting point

    46-48 ° C (lit.)

    Cov ntsiab lus dej

    <0.5%

     

    Ntxiv rau qhov raug oxidized los yog txo rau 2,5-dimethoxybenzoic acid, benzonitrile los yog benzyl cawv, 2,5-dimethoxybenzaldehyde nws tus kheej kuj muaj qhov tshwj xeeb daim ntawv thov nqi. Los ntawm kev cuam tshuam nrog cov tshuaj nrog ntau hom kev ua haujlwm, cov tshuaj molecules nrog cov qauv sib txawv thiab cov teebmeem sib txawv tuaj yeem tau txais. Parkinson's disease (PD) yog ib hom kab mob neurodegenerative, thiab nws cov tsos mob tseem ceeb muaj xws li cov leeg nqaij tremor, rigidity, txav tsis yooj yim, lub cev lub cev thiab lub cev tsis sib haum xeeb. Kev loj hlob ntxiv tseem yuav ua rau kev paub, kev nkag siab, kev nco tsis meej thiab pom tseeb dementia. Tam sim no, kev kho mob ntawm PD feem ntau suav nrog kev kho tshuaj, kev kho mob phais thiab kev kho noob. Hauv kev kho tshuaj, phenamidine tau pom tias muaj cov txiaj ntsig zoo ntawm PD, nrog cov tshuaj toxicity tsawg thiab kev nyab xeeb zoo, thiab cov synthesis ntawm phenamidine yuav tsum tau siv 2,5-dimethoxybenzaldehyde ua cov khoom pib.

    Raws li cov txheej txheem synthesis qhia nyob rau hauv cov ntaub ntawv, 2,5-dimethoxybenzaldehyde yog tsuas yog tau los ntawm reacting 1,4-dimethoxybenzene nrog ib tug formylation tus neeg sawv cev. Formylation cov neeg ua haujlwm suav nrog (1) sib xyaw ntawm 1,1-dichloromethyl ether thiab titanium tetrachloride; (2) sib tov ntawm N, N-dimethylformamide thiab phosphorus oxychloride, sib tov ntawm N, N-dimethylformamide thiab oxalyl chloride; (3) sib tov ntawm N, N-dimethylformamide thiab thionyl chloride los yog sib tov ntawm urotropine thiab magnesium chloride. Txawm li cas los xij, cov txheej txheem no yuav tsum tau siv ntau ntawm titanium tetrachloride, phosphorus oxychloride lossis thionyl chloride. Cov reagents no tsis ruaj khov thiab yooj yim decomposed, thiab ib tug loj npaum li cas ntawm hydrochloric acid gas raug tso tawm thaum lub sij hawm cov tshuaj tiv thaiv, uas tsis yog ib puag ncig tus phooj ywg thiab muaj cov kev xav tau siab rau cov txheej txheem ua haujlwm.

    Ib txoj kev tshiab synthesis tau raug npaj. Txoj kev no siv 1,4-dimethoxybenzene thiab formaldehyde ua raw cov ntaub ntawv, thiab ua ib tug photooxidative coupling cov tshuaj tiv thaiv nyob rau hauv lub xub ntiag ntawm oxygen thiab ib tug catalyst nyob rau hauv xiav lub teeb irradiation kom zoo synthesize 2,5-dimethoxybenzaldehyde. Txoj kev no siv cov pa oxygen lossis cua ua cov oxidant, tsis tsim cov pa roj acidic, thiab yog ib puag ncig zoo. Tsis tas li ntawd, txoj kev no siv cov cobalt pheej yig los ua ib qho catalyst, uas yog tus nqi qis thiab tsim nyog rau kev lag luam.

    25kgs / nruas, 9tons / 20'container
    25kgs / hnab, 20tons / 20'container

    Peb mob siab rau kev ua tau zoo, muab kev pabcuam rau cov neeg siv khoom”, vam tias yuav dhau los ua pab pawg kev koom tes zoo tshaj plaws thiab tus thawj tswj hwm kev lag luam rau cov neeg ua haujlwm, cov chaw muag khoom thiab cov neeg siv khoom, paub txog tus nqi sib koom thiab txuas ntxiv mus rau Kev Tshuaj Xyuas Zoo rau Kev Xa Khoom sai thiab Siab Purity CAS 93-02-7 2, 5-Dimethoxybenzaldehyde, Peb yuav muab cov khoom zoo tshaj plaws zoo tshaj plaws, muaj peev xwm ua tau zoo tshaj plaws ntawm cov nqi hnyav, rau txhua tus neeg siv khoom tshiab thiab qub nrog tag nrho cov kev pabcuam ntsuab zoo tshaj plaws.
    Kev soj ntsuam zoo rauTuam Tshoj Chemical Intermediates thiab Pharmaceutical Raw Materials, Vim muaj kev hloov pauv hauv daim teb no, peb koom nrog peb tus kheej rau hauv cov khoom lag luam nrog kev mob siab rau thiab kev tswj hwm zoo. Peb tuav lub sijhawm xa khoom raws sijhawm, tsim qauv tshiab, zoo thiab pob tshab rau peb cov neeg siv khoom. Peb lub moto yog xa cov kev daws teeb meem zoo hauv lub sijhawm teev tseg.


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